%0 Journal Article %1 Riccio2008 %A Riccio, Daniel %A Wood, Derrick C. %A Miller, James M. %D 2008 %J Journal of Chemical Education %K %N 7 %P 965 %R 10.1021/ed085p965 %T Using Single Drop Microextraction for Headspace Analysis with Gas Chromatography %U http://pubs.acs.org/doi/abs/10.1021/ed085p965 %V 85 %X Headspace (HS) gas chromatography (GC) is commonly used to analyze samples that contain non-volatiles. In 1996, a new sampling technique called single drop microextraction, SDME, was introduced, and in 2001 it was applied to HS analysis. It is a simple technique that uses equipment normally found in the undergraduate laboratory, making it ideal for instructional use, especially to illustrate HS analysis or as an alternative to solid-phase microextraction (SPME) to which it is very similar. The basic principles and practice of HS–GC using SDME are described, including a complete review of the literature. Some possible experiments are suggested using water and N-methylpyrrolidone (NMP) as solvents.

@article{Riccio2008, abstract = { Headspace (HS) gas chromatography (GC) is commonly used to analyze samples that contain non-volatiles. In 1996, a new sampling technique called single drop microextraction, SDME, was introduced, and in 2001 it was applied to HS analysis. It is a simple technique that uses equipment normally found in the undergraduate laboratory, making it ideal for instructional use, especially to illustrate HS analysis or as an alternative to solid-phase microextraction (SPME) to which it is very similar. The basic principles and practice of HS–GC using SDME are described, including a complete review of the literature. Some possible experiments are suggested using water and N-methylpyrrolidone (NMP) as solvents. }, added-at = {2011-10-01T00:40:05.000+0200}, author = {Riccio, Daniel and Wood, Derrick C. and Miller, James M.}, biburl = {https://www.bibsonomy.org/bibtex/29b7bca6aa0563dad31a27d1d57507745/afcallender}, doi = {10.1021/ed085p965}, eprint = {http://pubs.acs.org/doi/pdf/10.1021/ed085p965}, file = {Riccio2008.pdf:indexed\\Riccio2008.pdf:PDF}, groups = {public}, interhash = {2c0bc66e7afccf47168a95a01a1108df}, intrahash = {9b7bca6aa0563dad31a27d1d57507745}, journal = {Journal of Chemical Education}, keywords = {}, number = 7, pages = 965, timestamp = {2011-10-01T00:40:05.000+0200}, title = {Using Single Drop Microextraction for Headspace Analysis with Gas Chromatography}, url = {http://pubs.acs.org/doi/abs/10.1021/ed085p965}, username = {afcallender}, volume = 85, year = 2008 }