%0 Journal Article %1 wu_shiftless_2008 %A Wu, Chin H %A Opella, Stanley J %D 2008 %J J Chem Phys %K Biomolecular,Carbon Isotopes,Leucine,Nitrogen Isotopes,Nuclear Magnetic Resonance %N 5 %P 52312 %R 10.1063/1.2816786 %T Shiftless nuclear magnetic resonance spectroscopy %V 128 %X The acquisition and analysis of high resolution one- and two-dimensional solid-state nuclear magnetic resonance (NMR) spectra without chemical shift frequencies are described. Many variations of shiftless NMR spectroscopy are feasible. A two-dimensional experiment that correlates the dipole-dipole and dipole-dipole couplings in the model peptide , (15)N labeled N-acetyl-leucine is demonstrated. In addition to the resolution of resonances from individual sites in a single crystal sample, the bond lengths and angles are characterized by the two-dimensional powder pattern obtained from a polycrystalline sample.

@article{wu_shiftless_2008, abstract = {The acquisition and analysis of high resolution one- and two-dimensional solid-state nuclear magnetic resonance (NMR) spectra without chemical shift frequencies are described. Many variations of shiftless NMR spectroscopy are feasible. A two-dimensional experiment that correlates the dipole-dipole and dipole-dipole couplings in the model peptide , (15)N labeled N-acetyl-leucine is demonstrated. In addition to the resolution of resonances from individual sites in a single crystal sample, the bond lengths and angles are characterized by the two-dimensional powder pattern obtained from a polycrystalline sample.}, added-at = {2017-03-14T02:48:56.000+0100}, author = {Wu, Chin H and Opella, Stanley J}, biburl = {https://www.bibsonomy.org/bibtex/285fe90a491691eb6c7958195e6d66fde/nmrresource}, doi = {10.1063/1.2816786}, interhash = {9b92c9a4a524f0a3573fb793f4be59fc}, intrahash = {85fe90a491691eb6c7958195e6d66fde}, issn = {0021-9606}, journal = {J Chem Phys}, keywords = {Biomolecular,Carbon Isotopes,Leucine,Nitrogen Isotopes,Nuclear Magnetic Resonance}, month = feb, number = 5, pages = 52312, pmid = {18266429}, timestamp = {2017-03-14T02:49:21.000+0100}, title = {{Shiftless nuclear magnetic resonance spectroscopy}}, volume = 128, year = 2008 }