Highly air stable FeCo nanocrystals were synthesized by the proteic
sol-gel method using a rotary oven. The synthesized materials were
characterized by TG, DTA, XRD, TPR, VSM, Mossbauer spectroscopy and
FEG-SEM. The results showed the effect of temperature and the influence
of the hydrogen flow rate on the formation of pure FeCo alloy and on the
average crystallite size. The use of a rotary oven is efficient,
directly influencing the homogeneity and the purity of the FeCo alloy.
The synthesized alloy has high values of saturation magnetization
according to the VSM results. The performed characterizations confirmed
that the synthetic route is interesting in the formation of FeCo alloy
nanocrystallites with high chemical stability. (C) 2014 Elsevier B.V.
All rights reserved.
%0 Journal Article
%1 WOS:000345749500064
%A Braga, Tiago Pinheiro
%A Dias, Diego Felix
%A de Sousa, Matheus Falcao
%A Soares, Joao Maria
%A Sasaki, Jose Marcos
%C PO BOX 564, 1001 LAUSANNE, SWITZERLAND
%D 2015
%I ELSEVIER SCIENCE SA
%J JOURNAL OF ALLOYS AND COMPOUNDS
%K Alloy; High Nanoparticles; stability} {FeCo;
%P 408-417
%R 10.1016/j.jallcom.2014.10.074
%T Synthesis of air stable FeCo alloy nanocrystallite by proteic sol-gel
method using a rotary oven
%V 622
%X Highly air stable FeCo nanocrystals were synthesized by the proteic
sol-gel method using a rotary oven. The synthesized materials were
characterized by TG, DTA, XRD, TPR, VSM, Mossbauer spectroscopy and
FEG-SEM. The results showed the effect of temperature and the influence
of the hydrogen flow rate on the formation of pure FeCo alloy and on the
average crystallite size. The use of a rotary oven is efficient,
directly influencing the homogeneity and the purity of the FeCo alloy.
The synthesized alloy has high values of saturation magnetization
according to the VSM results. The performed characterizations confirmed
that the synthetic route is interesting in the formation of FeCo alloy
nanocrystallites with high chemical stability. (C) 2014 Elsevier B.V.
All rights reserved.
@article{WOS:000345749500064,
abstract = {Highly air stable FeCo nanocrystals were synthesized by the proteic
sol-gel method using a rotary oven. The synthesized materials were
characterized by TG, DTA, XRD, TPR, VSM, Mossbauer spectroscopy and
FEG-SEM. The results showed the effect of temperature and the influence
of the hydrogen flow rate on the formation of pure FeCo alloy and on the
average crystallite size. The use of a rotary oven is efficient,
directly influencing the homogeneity and the purity of the FeCo alloy.
The synthesized alloy has high values of saturation magnetization
according to the VSM results. The performed characterizations confirmed
that the synthetic route is interesting in the formation of FeCo alloy
nanocrystallites with high chemical stability. (C) 2014 Elsevier B.V.
All rights reserved.},
added-at = {2022-05-23T20:00:14.000+0200},
address = {PO BOX 564, 1001 LAUSANNE, SWITZERLAND},
author = {Braga, Tiago Pinheiro and Dias, Diego Felix and de Sousa, Matheus Falcao and Soares, Joao Maria and Sasaki, Jose Marcos},
biburl = {https://www.bibsonomy.org/bibtex/271c10143d742e4fa2e076ad8868c885a/ppgfis_ufc_br},
doi = {10.1016/j.jallcom.2014.10.074},
interhash = {acb12a707243db5f53f752562f087a31},
intrahash = {71c10143d742e4fa2e076ad8868c885a},
issn = {0925-8388},
journal = {JOURNAL OF ALLOYS AND COMPOUNDS},
keywords = {Alloy; High Nanoparticles; stability} {FeCo;},
pages = {408-417},
publisher = {ELSEVIER SCIENCE SA},
pubstate = {published},
timestamp = {2022-05-23T20:00:14.000+0200},
title = {Synthesis of air stable FeCo alloy nanocrystallite by proteic sol-gel
method using a rotary oven},
tppubtype = {article},
volume = 622,
year = 2015
}