%0 Journal Article %1 grant_efficient_2007 %A Grant, Christopher V %A Sit, Siu-Ling %A De Angelis, Anna A %A Khuong, Kelli S %A Wu, Chin H %A Plesniak, Leigh A %A Opella, Stanley J %D 2007 %J J. Magn. Reson. %K Apoptosis,Biomolecular,Cyclic,Equipment Design,Intracellular Isotopes Magnetic Membranes,Nuclear Resonance,Peptides,Phosphorus %N 2 %P 279--284 %R 10.1016/j.jmr.2007.06.016 %T An efficient (1)\H\/(31)\P\ double-resonance solid-state \NMR\ probe that utilizes a scroll coil %V 188 %X The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of (1)H and (31)P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.

@article{grant_efficient_2007, abstract = {The construction and performance of a scroll coil double-resonance probe for solid-state NMR on stationary samples is described. The advantages of the scroll coil at the high resonance frequencies of (1)H and (31)P include: high efficiency, minimal perturbations of tuning by a wide range of samples, minimal RF sample heating of high dielectric samples of biopolymers in aqueous solution, and excellent RF homogeneity. The incorporation of a cable tie cinch for mechanical stability of the scroll coil is described. Experimental results obtained on a Hunter Killer Peptide 1 (HKP1) interacting with phospholipid bilayers of varying lipid composition demonstrate the capabilities of this probe on lossy aqueous samples.}, added-at = {2017-03-14T02:48:56.000+0100}, author = {Grant, Christopher V and Sit, Siu-Ling and {De Angelis}, Anna A and Khuong, Kelli S and Wu, Chin H and Plesniak, Leigh A and Opella, Stanley J}, biburl = {https://www.bibsonomy.org/bibtex/2dc00f9b7264659ad99abd988c276881c/nmrresource}, doi = {10.1016/j.jmr.2007.06.016}, interhash = {7bb0c849861d5976fe5c61ac70fcc1c9}, intrahash = {dc00f9b7264659ad99abd988c276881c}, issn = {1090-7807}, journal = {J. Magn. Reson.}, keywords = {Apoptosis,Biomolecular,Cyclic,Equipment Design,Intracellular Isotopes Magnetic Membranes,Nuclear Resonance,Peptides,Phosphorus}, month = oct, number = 2, pages = {279--284}, pmid = {17719813}, timestamp = {2017-03-14T02:49:21.000+0100}, title = {{An efficient (1){\{}H{\}}/(31){\{}P{\}} double-resonance solid-state {\{}NMR{\}} probe that utilizes a scroll coil}}, volume = 188, year = 2007 }